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Das Oligomerenproblem Bei Polyesterfasern
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ISBN10: 3531025260
ISBN13: 9783531025261
Publisher: Vs Verlag Fur Sozialwissenschaften
Published: Jan 1 1976
Pages: 65
Weight: 0.29
Height: 0.15 Width: 6.69 Depth: 9.61
Language: German
ISBN13: 9783531025261
Publisher: Vs Verlag Fur Sozialwissenschaften
Published: Jan 1 1976
Pages: 65
Weight: 0.29
Height: 0.15 Width: 6.69 Depth: 9.61
Language: German
1. Einleitung 4 2. Stand der Forschung 7 2. 1 Analytik 8 2. 2 Oligomerenaustritt beim Färben 10 3. Problemstellung 14 4. Ergebnisse 15 4. 1 Analytik 15 4. 1. 1 Dünnschichtchromatographie 16 4. 1. 2 Der Gesamtoligomerengehalt 17 4. 1. 3 Der Oberflächengehalt 17 4. 1. 4 Säulenchromatographie 19 4. 1. 5 Analytik von oligomerenhaltigen Ablagerungen 23 4. 2 Das Verhalten der Polyesteroligomere unter Färbebedingungen 24 4. 2. 1 Die Zeitabhängigkeit des Oligomerenaustritts 25 4. 2. 2 Die Abhängigkeit des Oberflächengehaltes von der Färbetemperatur und den zugesetzten Hilfsmitteln 26 4. 2. 3 Das cyclische Trimere als Dispersionsfarbstoff 28 4. 2. 4 Löslichkeit des cyclischen Trimeren in Wasser 32 4. 2. 5 Die Entstehung des Oberflächengehaltes an cyclischem Trimeren beim Färben 33 4. 2. 6 Der Einflu von Dispergiermitteln und des Hei ablassens der Flotte auf den Oberfläch- gehalt 34 4. 2. 7 Variation der Flottengeschwindigkeit und reduktive Nachreinigung 37 5. Diskussion 42 Analytik 42 5. 1 5. 2 Das Verhalten der Polyesteroligomere unter Färbebedingungen 43 6. Experimenteller Teil 46 6. 1 Eingesetzte Materialien 46 6. 1. 1 POlyester 46 6. 1 . 2 Oligomere 46 6. 2 UV-spektroskopische Untersuchungen 46 6. 3 Dünnschichtchromatographie 47 6. 4 Bestimmung des Gesamtgehalts 47 47 6. 4. 1 UV-spektroskopisch 6. 4. 2 Bestimmung durch Säulenchromatographie unter Druck 47 6. 5 Bestimmung des Oberflächengehalts 48 48 6. 5. 1 UV-spektroskopisch 6. 5. 2 Säulenchromatographische Bestimmung unter Druck 48 6. 6 Säulenchromatographie unter Druck (HPLC) 48 6.
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