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Mechanismusbasiertes Entdecken in Der Photoredoxkatalyse: Lumineszenzlöschung ALS Hilfsmittel Zur Entwicklung Von Photoredoxreaktionen
Paperback
Series: Bestmasters
ISBN13: 9783658172657
Publisher: Springer Spektrum
Published: Feb 15 2017
Pages: 129
Weight: 0.41
Height: 0.32 Width: 5.83 Depth: 8.27
Language: German
Michael Teders beschreibt einen konzeptionell neuartigen, mechanismusbasierten Screeningansatz zur Beschleunigung der Entdeckung photokatalytischer Reaktionen. Im Unterschied zu herkömmlichen Screeningmethoden, in denen die gesamte Reaktion betrachtet wird, analysiert der Autor bei diesem Ansatz nur einen einzelnen mechanistischen Schritt einer katalytischen Reaktion. Durch Verwendung von Lumineszenzspektroskopie zur Aufdeckung des Quenching-Schlüsselschritts identifiziert er in einem initialen Screening von 100 Komponenten zwei vielversprechende Substratklassen. Ein zweites, fokussierteres Screening liefert ihm mechanistische Einblicke, die er zur Entwicklung von Proof-of-Concept-Reaktionen verwendet. Zusammenfassend erleichtert diese schnelle und intuitive Herangehensweise die Entdeckung und Entwicklung neuer photokatalytischer Reaktionen.
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